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51.
基于聚四氟乙烯(PTFE)微孔膜滤料扫描电镜(SEM)图像,建立PTFE微孔膜滤料微观结构模型,采用计算流体力学和离散单元法(CFD?DEM)耦合的方法对黏性颗粒在微孔膜滤料表面沉积特性进行模拟,引入液桥力模型,忽略范德华力的作用,统计计算域内颗粒的受力情况,分析了不同表面能条件下3~6 ?m粒径颗粒在微孔膜滤料表面的沉积特性,将模拟结果与黏附效率的经验公式进行对比。结果表明,黏附效率与经验值、颗粒受力与液桥力模型的相对误差均在6%以内,CFD?DEM耦合计算方法可用于模拟不同环境湿度条件下的颗粒沉积;过滤风速、粒径与黏性是影响沉积形态的重要因素,提高过滤风速及增大颗粒粒径与黏性,颗粒更易在滤料表面形成稳定的树突结构,黏附效率及含尘压降增加。环境相对湿度影响两物体间液桥体积,接触力影响颗粒沉积,当增加表面能与液桥体积时,接触力及液桥力均相应增加,根据受力平衡原理,环境相对湿度对颗粒沉积影响很大。 相似文献
52.
通过测量并分析引入气相前后D类颗粒间歇卸料过程中示踪颗粒的流动状态、压力分布和颗粒流率,发现床体内气固两相流动特性不仅随时间变化,还受到气速(正负压差)的影响。据此将卸料过程按时间分为3个阶段:初始蓄压(PS)阶段、稳定卸料(SD)阶段和非满管流(PP)阶段;并给出各卸料阶段不同正、负压差和重力条件下的气固流动特性。在时间较长、流场较为稳定的SD阶段,发现卸料口颗粒阻力是影响颗粒流率的关键参数,通过修正De Jong公式、Beverloo公式,依次建立卸料口颗粒阻力、D类颗粒卸料流率预测模型,与实验值吻合较好,有望为引入气相调控D类颗粒卸料流率的方法提供参考。 相似文献
53.
54.
Xu Sang Huimin Zhang Aiming Chang Junyi Zhou Haibing Li Xiaohui Li 《Journal of the American Ceramic Society》2020,103(3):1903-1911
The effects of different sintering temperatures on the system of Ba0.5Sr0.5TiO3–La0.8Ca0.2MnO3 (BST-LCM) material were investigated by means of scanning electron microscopy, X-ray, resistance-temperature measurements, and X-ray photoelectron spectroscopy. X-ray diffraction and X-ray photoelectron spectroscopy confirm that BST-LCM is completely miscible and BST is the main phase, which under the premise of following the theory of small polaron conduction, titanium ions interact with manganese ions, which affects the electrical properties of the system of BST-LCM material. For the electrical properties of related, the LCM content is inversely proportional to the activation energy. Through the linear fitting of the experimental data, the empirical formula between the sintering temperature B value and the content of solid solution is obtained, and the approximate B value within a certain range can be preliminarily calculated. 相似文献
55.
Pavel P. Fedorov Vera Y. Proydakova Sergey V. Kuznetsov Valery V. Voronov Alexandr A. Pynenkov Konstantin N. Nishchev 《Journal of the American Ceramic Society》2020,103(5):3390-3400
The thermal analysis and X-ray powder diffraction studies of the Li2SO4–Na2SO4 system, including the high-temperature X-ray diffraction technique, have elucidated four phases of variable composition: three solid solutions based on the α-Li2SO4, α-Na2SO4, and α-LiNaSO4 high-temperature polymorphs, and a low-temperature β-LiNaSO4 phase. α-Na2SO4-Base solid solution disintegrates into two phases via a monotectoid phase transformation. It is quite probable that the monotectoid process is related to the conversion of the second-order phase transition to the first-order phase transition. 相似文献
56.
Makrina A. Chairopoulou Fabian Kratzer Roland Gross Michael Herrmann Ulrich Teipel 《化学工程与技术》2020,43(5):904-912
Thermogravimetric analysis of a coccolith-containing biogenic broth showed a three-step degradation process. According to this system behavior, the biogenic broth was heated to specific temperatures and characterized in terms of its morphology, surface chemistry, and crystallinity. The elemental and organic composition of the treated samples was also evaluated and compared to the reference material. The presented results were acquired in an effort to exploit pretreatment scenarios for such a biogenic system that would improve and support a separation process. 相似文献
57.
采用固定床反应器分别探究了三类催化剂(固体磷酸催化剂、酸性阳离子交换树脂催化剂以及分子筛催化剂)对异丁烯齐聚过程的影响。实验结果表明:固体磷酸催化剂适用于C8烯烃的生产,酸性阳离子树脂催化剂及改性的分子筛催化剂(Hβ)适合生产C12烯烃。异丁烯齐聚产物C8~C16(清洁燃料油)因无芳烃、无硫,在石化工业中具有非常广泛的应用潜力;由三种类催化剂的评价结果来看,C8~C16的选择性最高时均能接近100%,但是固体磷酸催化剂和酸性阳离子树脂催化剂的异丁烯原料转化率比Hβ分子筛催化剂低,Hβ催化作用下异丁烯转化率可以达到88%。 相似文献
58.
《International Journal of Hydrogen Energy》2020,45(22):12459-12475
Thermal effects in a H2O and CO2 assisted tubular direct carbon solid oxide fuel cell (DC-SOFC) are numerically investigated. Parametric simulations are further conducted to study the effects of operating potential, the distance between carbon and anode, inlet gas temperature, and anode inlet gas flow rate on the thermal behaviors of the fuel cell. It is found that the fuel cell with H2O as gasification agent performs considerably better than the cell with CO2 as gasification agent in all cases. It is also found that the temperature field of the fuel cell is highly uneven. The breakdown of the heat sources in the fuel cell shows that the H2O assisted DC-SOFC has much higher heat generation and consumption than the CO2 assisted cell. Interestingly, a thermal neutral voltage is observed, at which no heating or cooling of the cell is needed. In addition, the distance between the anode and the carbon layer is required to be as small as possible, which improves the temperature uniformity of the fuel cell. The results of this study demonstrates the importance of thermal effects in DC-SOFCs and form a solid foundation for DC-SOFC thermal management. 相似文献
59.
O.N. Kondrateva G.E. Nikiforova A.V. Tyurin M.A. Ryumin V.M. Gurevich A.P. Kritskaya K.S. Gavrichev 《Ceramics International》2018,44(15):18103-18107
The heat capacity of ytterbium orthovanadate was first measured by adiabatic calorimetry in the temperature range T?=?12.28–344.06?K. No obvious anomalies were observed on the curve obtained. The values of standard thermodynamic functions in the temperature range T?=?0–400 K were calculated. Based on low-temperature calorimetry data obtained, previously published data on the high-temperature heat capacity of ytterbium orthovanadate were corrected. The anomalous contribution to heat capacity for YbVO4 was compared with the data known for YbPO4. 相似文献
60.
Thermodynamically stable (Hf1–xTax)C (x?=?0.1–0.3) compositions were selected by First Principle Calculation and synthesized in nanopowders via high-energy ball milling and carbothermal reduction of commercial oxides at 1450?°C. The formation of a solid solution during powder synthesis was investigated. The solid solution carbide powders were sintered at 1900?°C by spark plasma sintering without a sintering aid. As a result, the (Hf1–xTax)C solid solution carbides exhibited high densities, excellent hardness and fracture toughness (ρ: 98.7–100.0%, HVN: 19.69–19.98?GPa, KIC: 5.09–5.15?MPa?m1/2) compared with previously reported HfC and HfC–TaC solid solution carbides. 相似文献